A sample of coal was analyzed as follows: Exactly was weighed into silica crucible. After heating for one hour at 110°C, the residue weighed The crucible next was covered with a vented lid and strongly heated for exactly seven minutes at 950 = 20° C. ... Solution: Weight of coal taken = gm Mass of moisture in coal = ...
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by heating an airdried coal sample at 105 ... (Btu/lb dry) OF THE INDIANA DANVILLE COAL Source: M. Mastalerz, A Drobniak, J. Rupp and N. Shaffer, "Assessment of the Quality of Indiana coal for Integrated Gasification Combined Cycle Performance (IGCC)', Indiana Geological Survey, Indiana University, June 2005
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Dry Basis (d) the condition in which the sample is assumed to be completely free of moisture. Dry, AshFree Basis (daf) a hypothetical condition for which the sample is assumed to be completely free of moisture and ash. This allows a judgement based on only the organic component of the coal.
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Typical comparison of readsorption curves between the ovendried coal sample and blending of the hot oven (150 C) dried coal sample (500 g) with 200 g of raw (airdried) coal sample.
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Chemical/Atmospheric or dry corrosion occurs mainly by, direct attack of atmospheric gases such as O2, CO2, H2S, halogens, SO2 etc. on the surface of metals. The metal forms corresponding compounds such as oxides, carbonates, sulphides, halides or sulphates. The action of some organic or anhydrous
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Moisture in airdried laboratory analysis sample if coal and coke It is the moisture in coal which has been airdried under the laboratory atmospheric condition prior to analysis and is determined as a part of proximate analysis and also whenever portions of sample arc weighed later for other analysis and tests. ...
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belonging to different Indian coal fields. ... Where GCV in kcal/kg and moisture, ash, fixed carbon in air dried percentage basis. In the present study, 49 samples were used to develop the regression model and 10 were used to ... required sample of small sizes (1 to 10 g) range and it has utility when results on one sample are (%) (%) (%) (%)
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• Dry basis (d): The basis for analytical data calculated to a theoretical basis of no moisture associated with the sample. The numerical value as established in ASTM D3173 or D7582 is used for converting the asdetermined data to a dry basis.
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ADB AirDried Basis. In coal sample analysis, ADB neglects the presence of moistures other than inherent moisture while DB (drybasis) leaves out all moistures, including surface moisture, inherent moisture, and other moistures. ARB AsReceived Basis. In coal sample analysis, ARB puts all variables into consideration and uses the total ...
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Allow the sample in the air drying cabinet Mix or stir from time to time being careful not to lose and coal particles till weight loss is less than %/h. Record the weight of the tray + sample after air drying cabinet. STAGE II (Residual Moisture) Heat the empty dish at 107 ±3°C and weigh after colling. Pass the air dried sample through 250 ...
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where M ad represents the airdrying base moisture, %; m and m 1 are the coal sample weight and its lost after the drying, g. The equilibrium moisture ( M e ) is defined as the moisture content when the pore water in the coal sample with ∼ mm pores reaches saturation at a temperature of 30°C and a relative humidity of 96% (using a ...
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ADM is Air Dried Moisture (Moisture in the Analysis Sample) NM is Nominated Moisture AR is As Received Basis AD is As Determined (Air Dried) Basis ... Two stage total moisture determination is used when the coal sample is too small mass or too wet to divide or crush without the potential of losing significant amounts of moisture. TMar, % = [Rm ...
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Before conducting the uniaxial compression test on the coal samples, all samples were first dried in a drying chamber at a temperature of 60°C for 48 h ; then, the coal samples of groups BD were saturated with water, and the changes in mass and moisture content with time after soaking are given in Figure 1. When the soaking time was longer ...
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The gain in calorific value was greater than the energy required to dry the coal samples, showing that a fluidized bed using moderately warm dry air is an energyefficient drying technology.
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The relative density is calculated from the displacement of the wetting agent by the coal sample using the equation below. Equation: RD = M a / (M a + M w M t) Where: M a = mass of coal in air. M w = mass of stoppered density bottle filled with water and wetting agent. M t = mass of coal, stopped density bottle filled with water and wetting ...
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If it is dried at 40℃, it is enough to cool normally for 3 hours, while, the oxidizing coal should not be dried at a temperature above 40 degrees centigrade. Coal Sample Reduction. Coal sample reduction is the process of reducing the size of coal samples, aiming at increasing the number of sample particles and decreasing the sample division bias.
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Air drying or drying in a nitrogen atmosphere can be used for either method, depending on the coal rank. Drying in a nitrogen atmosphere is suitable for all hard coals, while drying in air is suitable only for hard coals not susceptible to oxidation. 1. Singlestage the sample is crushed to a nominal topsize of mm.
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Take 100 gram of coal sample whose size is < mm keep this sample in lab for 24 hours at atmospheric condition. Then calculate the surface moisture = Loss in weight X 100 / Weight of the sample (100 gram) For example: After drying the 100 gram coal in lab for 24 hours its total becomes 92 gram then,
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Experimental Procedure : About 1g of finely pulverized 212 micron (BSS) airdried coal sample is weighed in a silica crucible and then placed within an electric hot air oven. It is maintained at 110o C. The crucible with the coal sample is allowed to put in the oven for hours and it is taken out with the help of tongues, and then cooled in ...
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r emissions, airdried or ovendried soils are commonly used in the laboratory. To date, few studies have compared the effects of different drying methods on soil N r gas fluxes and N fractions. Here, the authors studied soil water content, pH, (in)organic N content, and N r gas fluxes of airdried, freezedried, ovendried, and fresh soils
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1 Scope. This International Standard describes two methods for determination of the total moisture content of hard coals, a twostage method and a singlestage method. For either method there is a choice between drying in air and drying in a nitrogen atmosphere. Depending on the coal rank, there may be systematic differences between the results ...
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(5 marks) 6 (b) gm of air dried coal sample was taken in a crucible, after heating it in an electric oven at 110°C for 1 hr the residue was weighed gm. The residue was heated in Silica crucible covered with vented lid at a temperature 925±257°C for exactly 7 minutes. After cooling the weight of residue was found to contain gm.
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Definition :The analysis of coal in which percentages of C, H, N, S and O. elements are found out, is known as ultimate analysis. f Carbon and Hydrogen. Method for determination. A known weight of powdered and air dried coal sample is burnt in the. presence of pure oxygen, in a combustion apparatus. C and H are.
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Calculate results of proximate analysis. gm of air dried coal sample was taken in a silica crucible, after heating it in an electric oven at 1050∘C − 1100∘C 1050 ∘ C − 1100 ∘ C for 1 hour, the residue was weighed gm. The residue was heated in silica crucible covered with vented lid at temperature 950 − 9700∘C 950 − ...
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The coal is first finely ground and air dried. Samples of the dried coal are then subjected to several operations, with the sample weights being recorded before and after each operation. Moisture content is determined as the weight loss when a sample is held at 105°C in an oxygenfree atmosphere for roughly 2 hours, added to the weight loss ...
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ADM is Air Dried Moisture (Moisture in the Analysis Sample) NM is Nominated Moisture AR is As Received Basis AD is As Determined (Air Dried) Basis ... Two stage total moisture determination is used when the coal sample is too small mass or too wet to divide or crush without the potential of losing significant amounts of moisture. TMar, % = [Rm ...
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The ash yield of a coal sample is the amount of material remaining after combustion. For this test, a coal sample is ground to a set size (60 mesh, less than or equal to 250 micron particle size), weighed, and then combusted at temperatures between 500 and 750°C for 1 hour. ... Coals with volatile matter of 20 to 35 percent (on an airdried ...
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coal samples taken from the bulk material and not from the individual components. Given the extreme complexity of coal, coal sampling protocols must provide material that is representative of the lot sampled. To ensure a representative sample is collected, correct
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This practice 2 covers the reduction and division of gross or divided samples, and the preparation of composite samples, up to and including the individual portions for laboratory analysis. Reduction and division procedures are prescribed for coals of the following groups: Group A includes coals that have been cleaned in all sizes.
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